CTNF 18/288,076 CTNF 98404 DETAILED ACTION Notice of Pre-AIA or AIA Status 07-03-aia AIA 15-10-aia The present application, filed on or after March 16, 2013, is being examined under the first inventor to file provisions of the AIA. Claim Objections It is recommended that Applicant amend the claims as follows: In claim 14 , line 3, “conductive material comprises of a single-walled carbon nanotube” should read “conductive material comprises [[of]] a single-walled carbon nanotube” for clearer syntax. In claim 15 , line 2, it is recommended to change “the conductive material has an impurity content of 3000 ppm to 4000 ppm” to “ the conductive material has an the impurity content [[of]] is 3000 ppm to 4000 ppm” to clarify that such further limits parent claim 14’s impurity-content range (as clearly intended on p. 12, lines 10–12). Appropriate correction is required. Claim Rejections - 35 USC § 112 07-30-02 AIA The following is a quotation of 35 U.S.C. 112(b): (b) CONCLUSION.—The specification shall conclude with one or more claims particularly pointing out and distinctly claiming the subject matter which the inventor or a joint inventor regards as the invention. The following is a quotation of 35 U.S.C. 112 (pre-AIA), second paragraph: The specification shall conclude with one or more claims particularly pointing out and distinctly claiming the subject matter which the applicant regards as his invention. 07-34-01 Claim(s) 1–14 is/are rejected under 35 U.S.C. 112(b) or 35 U.S.C. 112 (pre-AIA), second paragraph, as being indefinite for failing to particularly point out and distinctly claim the subject matter which the inventor or a joint inventor (or for applications subject to pre-AIA 35 U.S.C. 112, the applicant), regards as the invention. Claim 1 recites “the positive electrode has an initial efficiency ratio of an initial discharge capacity to an initial charge capacity in the secondary battery using lithium as a counter electrode” in lines 19–21. As the “secondary battery” already includes the Si-containing active material as the negative/counter electrode, it is unclear if “the secondary battery” of line 20 references and further limits the “secondary battery” of the preamble or is meant to introduce a separate secondary battery including the positive electrode and lithium as a counter electrode. P. 9, lines 23–26, specially define the “initial efficiency ratio” as “a ratio of an initial discharge capacity to an initial charge capacity when the positive electrode and lithium metal are used as counter electrodes, a half-coin cell is manufactured using a carbonate-based electrolyte, and charging and discharging proceed at 0.2C to 4.2V to 2.5" Thus, a separate secondary battery is meant to be introduced, and, therefore, claim 1 will be interpreted to require that the “positive electrode has an initial efficiency ratio in [a separate] secondary battery using lithium as a counter electrode”. Claim 12 recites “the negative electrode has an initial efficiency ratio of an initial discharge capacity to an initial charge capacity in a secondary battery using lithium as a counter electrode” in lines 2 and 3. It is unclear whether this “secondary battery” and “lithium as a counter electrode” are meant to be the same as or different than claim 1’s “secondary battery using lithium as a counter electrode”, claim 1’s overall “secondary battery” in the preamble (particularly in light of above 112(b)), or some other (test) battery/counter electrode. P. 11, lines 8 and 9, specially define the negative electrode’s “initial efficiency” as being “the same as the described for the positive electrode … [but] lithium is used as the negative electrode and the counter electrode.” Thus, an additional, separate secondary battery is intended, and, therefore, for this Office Action claim 12 will be interpreted to require that the “negative electrode has an initial efficiency ratio … in [an additional, separate] secondary battery using lithium as a counter electrode”. The dependent claims fail to correct these deficiencies and are rejected likewise. Appropriate correction is required. 07-30-03-h AIA Claim Interpretation As noted above, the “initial efficiency” of each of the positive electrode and negative electrode (claims 1 and 12, respectively) will be interpreted according to their respective special definitions. Claim 7 recites “the lithium transition metal oxide is a single particle” in line 2. The “single particle” will be interpreted as “a state in which the primary particles exist individually, or less than 10 primary particles are aggregated,” as specially defined on p. 8, lines 21 and 22. Claim Rejections - 35 USC § 103 07-20-aia AIA The following is a quotation of 35 U.S.C. 103 which forms the basis for all obviousness rejections set forth in this Office action: A patent for a claimed invention may not be obtained, notwithstanding that the claimed invention is not identically disclosed as set forth in section 102, if the differences between the claimed invention and the prior art are such that the claimed invention as a whole would have been obvious before the effective filing date of the claimed invention to a person having ordinary skill in the art to which the claimed invention pertains. Patentability shall not be negated by the manner in which the invention was made. 07-23-aia AIA The factual inquiries for establishing a background for determining obviousness under 35 U.S.C. 103 are summarized as follows: 1. Determining the scope and contents of the prior art. 2. Ascertaining the differences between the prior art and the claims at issue. 3. Resolving the level of ordinary skill in the pertinent art. 4. Considering objective evidence present in the application indicating obviousness or nonobviousness. 07-20-02-aia AIA This application currently names joint inventors. In considering patentability of the claims the examiner presumes that the subject matter of the various claims was commonly owned as of the effective filing date of the claimed invention(s) absent any evidence to the contrary. Applicant is advised of the obligation under 37 CFR 1.56 to point out the inventor and effective filing dates of each claim that was not commonly owned as of the effective filing date of the later invention in order for the examiner to consider the applicability of 35 U.S.C. 102(b)(2)(C) for any potential 35 U.S.C. 102(a)(2) prior art against the later invention. 07-21-aia AIA Claim(s) 1– 13 is/a re rejected under 35 U.S.C. 103 as being unpatentable over Lee e t al. (US 20150228979 A1) (Lee) in view of Kuroda (JP 6633796 B1; citation to English equivalent US 20220059834 A1). Rega rding claims 1 and 3 , Lee discloses a secondary battery (LIB, ¶ 0117, 0118), comprising a positive electrode; a negative electrode; and a separator interposed between the positive electrode and the negative electrode (e.g., ¶ 0117), wherein the positive electrode comprises a positive electrode mixture layer on at least one surface of a positive electrode current collector (e.g., ¶ 0114, 0118), wherein the positive electrode mixture layer comprises a positive electrode active material comprising a lithium transition metal oxide (NCM, Id. ), wherein the negative electrode comprises a negative electrode mixture layer on at least one surface of a negative electrode current collector (e.g., ¶ 0115), wherein the negative electrode mixture layer comprises a negative electrode active material comprising a silicon-containing active material ( Id. ). Lee generally discloses that the lithium transition metal oxide positive electrode active material may be represented by Li x Co a Ni b M c O 2+α , where 0.9 < x < 1.5, 0 < a < 0.5, 0 < b < 1, 0 < c < 1, -0.1 ≤ α ≤ 0.1, and M comprises at least one element such as Mn, Al, or Zr (¶ 0020). Lee further discloses that the oxide should provide increased discharged capacity and improved lifespan characteristics (¶ 0045) as well as sufficient initial efficiency (¶ 0066), but Lee fails to explicitly disclose that the positive electrode active material is doped with a dopant, wherein a molar ratio of Ni is 88% or more based on a total amount of transition metals excluding Li present in the positive electrode active material. Kuroda teaches lithium Ni-based oxide positive active material (Title) designed to enhance positive electrode initial efficiency (¶ 0007, exs.). The material includes core particles and a coating material (¶ 0017), where the core is represented by Li[Li x (Ni 1–y–z–w )Co y Mn z M w ) 1–x ]O 2 , where -0.1 ≤ x ≤ 0.2, 0 ≤ y ≤ 0.4, 0 ≤ z ≤ 0.4, 0 ≤ w ≤ 0.1, and M is one or more of Fe, Cu, Ti, Mg, Al, W, B, Mo, Nb, Zn, Sn, Zr, Ga, La, and V (¶ 0040–0042), while the coating material contains element X, which may preferably be Zr (¶ 0017, 0124). Kuroda teaches that M in the core may preferably be Al for high cycle characteristics and thermal stability (¶ 0062, exs.). Further, x is preferably 0–0.1 from the viewpoint of high cycle characteristics and initial efficiency (¶ 0050); y is preferably 0–0.4 from the viewpoint of low internal resistance and thermal stability (¶ 0054); z is preferably 0–0.4 from the viewpoint of high cycle characteristics and storage stability at high temperature (¶ 0057); and w is preferably 0–0.1 from the viewpoint of low internal resistance and high discharge capacity (¶ 0063). Further, the coating element X is preferably 0.05–5 mol% based on the ratio of X/(Ni+Co+Mn+M) to further enhance the invention (¶ 0126). Moreover, in being included in a very small amount to modify the (semiconducting) oxide’s electrical/electrochemical properties, the element X such as Zr reasonably constitutes a (surface) “dopant,” absent special definition. Kuroda and Lee are analogous prior art to the claimed invention because they pertain to the same field of endeavor, namely Ni-containing positive electrode active material. It would have been obvious to one of ordinary skill in the art, before the effective filing date of the claimed invention, to adopt Kuroda’s material as Lee’s Ni-based oxide—such that the material would be “doped” with a dopant of Zr—with the reasonable expectation of achieving the desired initial efficiency, as taught by Kuroda. Regarding the requirement of ≥ 88 mol% Ni based on a total amount of transition metals excluding Li present in the positive electrode active material, although modified Lee may not explicitly disclose such, it would have been obvious to arrive at this range by routinely optimizing the above metals’ molar ratios to balance the above considerations like initial efficiency, high discharge capacity, thermal stability, and low internal resistance, as taught by Kuroda (MPEP 2144.05 (II)). Lee further discloses that the positive electrode has an initial efficiency ratio of an initial discharge capacity to an initial charge capacity in [a separate] secondary battery using lithium as a counter electrode of, e.g., 89.7% (Table 2, Ex. 3). Such is determined by manufacturing a half-cell using the positive electrode and Li metal alongside a carbonate-based electrolyte (¶ 0117, 0139) and subjecting the cell to constant-current charging of half-cell at 0.1C to 4.3V vs Li, constant-voltage charging until current reaches 0.01C, and then discharging at 0.1C until 3.0V vs Li (¶ 0140), substantially similar to spec. (e.g., p. 9, lines 23–26). Even if slightly outside the instant 85–89%, the skilled artisan would recognize that Lee’s 89.7% is so close to the instant range that each electrode would be expected to perform substantially similarly. Specifically, Lee includes 89.7% as one of the inventive examples (Table 2) and never appears to test below the instant 85% to determine that such is a poorer example. Further, the instant specification only tests comp. exs. at ≥ 90% (Comp. Exs. 1–3). Thus, absent demonstrated criticality, the skilled artisan would have expected substantially similar performance at Lee’s ~ 89.7% as within the instant 85–89% (MPEP 2144.05 (I)). Further, Lee generally discloses that the positive electrode’s initial efficiency may be ≤ 91.5%, most preferably ≤ 87%, because higher rates may reduce discharge capacity (¶ 0066). Such appears to overlap the recited 85–89% such that the skilled artisan could have routinely selected within the overlap with a reasonable expectation of forming a successful electrode with maintained discharge capacity (MPEP 2144.05 (I)). Regarding claim 2 , modified Lee discloses the secondary battery according to claim 1. Regarding the requirement that the lithium transition metal oxide is doped with the dopant in an amount of 4000 ppm to 5000 ppm based on a total weight of the lithium transition metal oxide, again, even though modified Lee may not explicitly articulate such, Kuroda clearly teaches a miniscule amount of element X/dopant (e.g., ¶ 0063, 0126), where the dopant must be contained in an amount sufficient to reduce internal resistance, but including too much dopant can hamper discharge capacity (¶ 0063). To balance these effects, then, it would have been obvious to arrive at the recited range by routinely optimizing the dopant’s wt% (MPEP 2144.05 (II)). Regarding claims 4–6 , modified Lee discloses the secondary battery according to claim 1. Regarding the requirement that the lithium transition metal oxide is represented by the formulae of claims 4 and 5 and that a is 0.90 ≤ a < 1 (claim 6), again, although modified Lee may not explicitly articulate such, Kuroda suggests balancing each metal’s molar ratio for considerations such as initial efficiency, high discharge capacity, thermal stability, and low internal resistance, as discussed above. As seen in Kuroda’s general formula, moreover, the molar ratios respectively overlap the instant formulae’s ratios, where M in instant formula 1/claim 4 would be Al (via M in Kuroda’s formula, as explained above). To ensure high cycle characteristics, sufficient initial efficiency, high thermal stability, low internal resistance, high storage stability at high temperature, and high discharge capacity, it would have been obvious to arrive at the recited formulae/molar ratios by routinely optimizing each metal’s ratio in Kuroda’s formula (MPEP 2144.05 (II)). Regarding claims 7 and 8 , modified Lee discloses the secondary battery according to claim 1, wherein the lithium transition metal oxide is a single particle (see one body—i.e., non-aggregated primary particles—NCM in Lee’s ¶ 0103 and 0114 and fig. 1) and has an average diameter D50 of preferably 3~5 μm (Lee, ¶ 0055), falling within 1–5 μm. Regarding claim 9 , modified Lee discloses the secondary battery according to claim 1. Again, Lee generally discloses a positive electrode’s initial efficiency of ≤ 91.5%, most preferably ≤ 87%, because higher rates may reduce discharge capacity (¶ 0066). Such appears to overlap the recited 86–87% such that the skilled artisan could have routinely selected within the overlap with a reasonable expectation of forming a successful electrode with maintained discharge capacity (MPEP 2144.05 (I)). Regarding claims 10 and 11 , modified Lee discloses the secondary battery according to claim 1, wherein the negative electrode active material further comprises a carbon-containing material (graphite in Lee’s ¶ 0115), and the silicon-containing active material is present in an amount of 10% by weight based on a total weight of the negative electrode active material (see 90:10 graphite:SiOx weight ratio in Lee’s ¶ 0115), falling within 1–10%. Regarding claim 12 , modified Lee discloses the secondary battery according to claim 1. Similar to above, Lee embodies a negative electrode initial efficiency of, e.g., 85% (Table 2, Exs. 1–3), which appears to be determined substantially similarly as the instant specification (compare Lee’s ¶ 0141 to spec.’s p. 11, lines 8 and 9). Even if, arguendo , this range fell slightly outside 85–89% based on the slight discrepancies in (dis)charging current and voltage between Lee and the instant disclosure, the skilled artisan would recognize that Lee’s ~ 85% is so close to the instant range that the two electrodes would be expected to perform substantially similarly. Specifically, Lee includes 85% in the inventive examples versus comp. exs. at, e.g., 81% and 79% (Table 2), and the instant specification purports no criticality to 85–89%. Thus, absent demonstrated criticality, the instant range is considered merely an obvious variant of Lee’s (MPEP 2144.05 (I)). More generally, however, Lee discloses that the anode’s initial efficiency may be ≤ about 88.0% because this range allows the cathode with low initial efficiency to be used without any loss in discharge capacity (¶ 0068). It would have been obvious to routinely select within the apparent overlap with a reasonable expectation of forming a successful negative electrode with maintained discharge capacity (MPEP 2144.05 (I)). Regarding claim 13 , modified Lee discloses the secondary battery according to claim 12. Again, even if Lee’s ~ 85% falls slightly outside 86 to 87%, the skilled artisan would have expected substantially similar performance from Lee’s electrode as the instant spec.’s given how close these values are and without any demonstrated criticality, as discussed above. Further, based on Lee’s broader ≤ 88.0%, it would have been obvious to select within the apparent overlap with a reasonable expectation of forming a successful negative electrode with maintained discharge capacity (MPEP 2144.05 (I)) . 07-21-aia AIA Claim (s) 14 and 15 is/are rejected under 35 U.S.C. 103 as being unpatentable over Lee et al. (US 20150228979 A1) (Lee) in view of Kuroda (JP 6633796 B1; citation to English equivalent US 20220059834 A1), as applied to claim 1, further in view of Dillon et al. (US 20020081380 A1, from 10/24/23 IDS) (Dillon) . Regarding claims 14 and 15 , modified Lee discloses the secondary battery according to claim 1, wherein the positive electrode mixture layer further comprises a conductive material (Lee, e.g., ¶ 0072, 0114). Lee further discloses that the conductive material is not limited and lists carbon nanotubes as one possibility (¶ 0073) but fails to explicitly disclose that the conductive material comprises [[of]] a single-walled carbon nanotube having an impurity content of 300–5000 ppm (claim 14) or 3000–4000 ppm (claim 15). Dillon teaches highly pure SWCNTs for applications in, e.g., batteries due to their unique electronic, optical, and mechanical properties (Abstract, ¶ 0004). Dillon recognizes that SWCNTs often include impurities such as metals and non-nanotube carbon fractions, and high-purity SWCNTs must be produced before the nanotubes’ advantages can be effectively realized (¶ 0004). Dillon teaches SWCNTs with purity ≥ 98 wt% and with metal content < 0.5 wt% (¶ 0055). Dillon is analogous prior art to the claimed invention because they are reasonably pertinent to a problem the inventor would have faced, namely selecting a suitable conductive material for the positive electrode mixture layer. It would have been obvious to one of ordinary skill in the art, before the effective filing date of the claimed invention, to employ Dillon’s SWCNTs as Lee’s positive electrode conductive material with the reasonable expectation of achieving high-purity nanotubes with effectively realized electronic, optical, and mechanical properties, as taught by Dillon. The metal content < 0.5 wt% yields an impurity content < 5000 ppm. This range overlaps claim 14’s 300–5000 ppm with sufficient specificity to satisfy this range given the specification’s apparent lack of criticality (MPEP 2131.03 (II)). Moreover, this range significantly overlaps claim 15’s 3000–4000 ppm such that the skilled artisan could have routinely selected within the overlap with a reasonable expectation of forming a successful SWCNT with minimal impurities and advantageous properties (MPEP 2144.05 (I)). Double Patenting 08-33 AIA The nonstatutory double patenting rejection is based on a judicially created doctrine grounded in public policy (a policy reflected in the statute) so as to prevent the unjustified or improper timewise extension of the “right to exclude” granted by a patent and to prevent possible harassment by multiple assignees. A nonstatutory double patenting rejection is appropriate where the conflicting claims are not identical, but at least one examined application claim is not patentably distinct from the reference claim(s) because the examined application claim is either anticipated by, or would have been obvious over, the reference claim(s). See, e.g., In re Berg , 140 F.3d 1428, 46 USPQ2d 1226 (Fed. Cir. 1998); In re Goodman , 11 F.3d 1046, 29 USPQ2d 2010 (Fed. Cir. 1993); In re Longi , 759 F.2d 887, 225 USPQ 645 (Fed. Cir. 1985); In re Van Ornum , 686 F.2d 937, 214 USPQ 761 (CCPA 1982); In re Vogel , 422 F.2d 438, 164 USPQ 619 (CCPA 1970); In re Thorington , 418 F.2d 528, 163 USPQ 644 (CCPA 1969). A timely filed terminal disclaimer in compliance with 37 CFR 1.321(c) or 1.321(d) may be used to overcome an actual or provisional rejection based on nonstatutory double patenting provided the reference application or patent either is shown to be commonly owned with the examined application, or claims an invention made as a result of activities undertaken within the scope of a joint research agreement. See MPEP § 717.02 for applications subject to examination under the first inventor to file provisions of the AIA as explained in MPEP § 2159. See MPEP § 2146 et seq. for applications not subject to examination under the first inventor to file provisions of the AIA. A terminal disclaimer must be signed in compliance with 37 CFR 1.321(b). The filing of a terminal disclaimer by itself is not a complete reply to a nonstatutory double patenting (NSDP) rejection. A complete reply requires that the terminal disclaimer be accompanied by a reply requesting reconsideration of the prior Office action. Even where the NSDP rejection is provisional the reply must be complete. See MPEP § 804, subsection I.B.1. For a reply to a non-final Office action, see 37 CFR 1.111(a). For a reply to final Office action, see 37 CFR 1.113(c). A request for reconsideration while not provided for in 37 CFR 1.113(c) may be filed after final for consideration. See MPEP §§ 706.07(e) and 714.13. The USPTO Internet website contains terminal disclaimer forms which may be used. Please visit www.uspto.gov/patent/patents-forms. The actual filing date of the application in which the form is filed determines what form (e.g., PTO/SB/25, PTO/SB/26, PTO/AIA/25, or PTO/AIA/26) should be used. A web-based eTerminal Disclaimer may be filled out completely online using web-screens. An eTerminal Disclaimer that meets all requirements is auto-processed and approved immediately upon submission. For more information about eTerminal Disclaimers, refer to www.uspto.gov/patents/apply/applying-online/eterminal-disclaimer . Claim(s) 1, 3–6, and 10 is/are provisionally rejected on the ground of nonstatutory double patenting as being unpatentable over claim(s) 11, 12, 14, and 15 of copending Application 18/559673 (reference application, published as US 20250300224 A1). Although the claims at issue are not identical, they are not patentably distinct from each other as follows: Ref. claims 11, 12, 14, and 15 together encompass instant claim 1 (noting that positive and negative electrode current collectors would be necessarily present to collect/distribute current), where the negative electrode active material may be a silicon-containing active material, the positive electrode active material comprises a lithium transition metal oxide, and the positive electrode’s initial efficiency—specially defined the same as in the instant spec. (see ref.’s ¶ 0093)—is 85–89%. More specifically, ref. claim 12 recites a general formula of the lithium metal oxide of Li 1+e (Ni a Co b Mn c M d )O 2 , where M is a dopant such as W, Zr, Al, or Nb; 0.85 ≤ a < 1; 0 < b ≤ 0.15; 0 < c ≤ 0.15; 0 ≤ d ≤ 0.1; and a + b + c + d = 1. This “a”/Ni content overlaps the instant ≥ 88 mol% Ni such that the skilled artisan could have routinely selected within the overlap with a reasonable expectation of forming a successful metal oxide with sufficient Ni content (MPEP 2144.05 (I)). Further, as discussed above, the ref.’s dopant may be Zr, reading on instant claim 3. Moreover, as seen above, the ref.’s general formula’s molar ratios overlap the instant ratios such that the skilled artisan could have arrived at instant claim 4–6’s formulae/ratios by routinely selecting within each overlap with a reasonable expectation of forming a successful lithium metal oxide (MPEP 2144.05 (I)). Further, ref. claim 15’s carbon material reads on instant claim 10. This is a provisional nonstatutory double patenting rejection because the patentably indistinct claims have not been patented. Conclusion 07-96 The cited art made of record and not relied upon is considered pertinent to applicant's disclosure: WO 2019163483 A1 (with citation to English equivalent US 20210050588 A1), US 20160197340, and US 20140272551 A1 all recognize lower-initial-efficiency positive electrodes and/or differences in initial efficiency between positive and negative electrodes, as well as ability to include Ni-based lithium oxide positive active materials and Si- and C-based negative active materials. Any inquiry concerning this communication or earlier communications from the examiner should be directed to JOHN S MEDLEY whose telephone number is (703)756-4600. The examiner can normally be reached 8:00–5:00 EST M–Th and 8:00–12:00 EST F. Examiner interviews are available via telephone, in-person, and video conferencing using a USPTO supplied web-based collaboration tool. To schedule an interview, applicant is encouraged to use the USPTO Automated Interview Request (AIR) at http://www.uspto.gov/interviewpractice. If attempts to reach the examiner by telephone are unsuccessful, the examiner’s supervisor, Jonathan Leong, can be reached on 571-270-192. The fax phone number for the organization where this application or proceeding is assigned is 571-273-8300. Information regarding the status of published or unpublished applications may be obtained from Patent Center. Unpublished application information in Patent Center is available to registered users. To file and manage patent submissions in Patent Center, visit: https://patentcenter.uspto.gov. Visit https://www.uspto.gov/patents/apply/patent-center for more information about Patent Center and https://www.uspto.gov/patents/docx for information about filing in DOCX format. For additional questions, contact the Electronic Business Center (EBC) at 866-217-9197 (toll-free). If you would like assistance from a USPTO Customer Service Representative, call 800-786-9199 (IN USA OR CANADA) or 571-272-1000. /J.S.M./Examiner, Art Unit 1751 /JONATHAN G LEONG/Supervisory Patent Examiner, Art Unit 1751 5/7/2026 Application/Control Number: 18/288,076 Page 2 Art Unit: 1751 Application/Control Number: 18/288,076 Page 3 Art Unit: 1751 Application/Control Number: 18/288,076 Page 4 Art Unit: 1751 Application/Control Number: 18/288,076 Page 5 Art Unit: 1751 Application/Control Number: 18/288,076 Page 6 Art Unit: 1751 Application/Control Number: 18/288,076 Page 7 Art Unit: 1751 Application/Control Number: 18/288,076 Page 8 Art Unit: 1751 Application/Control Number: 18/288,076 Page 9 Art Unit: 1751 Application/Control Number: 18/288,076 Page 10 Art Unit: 1751 Application/Control Number: 18/288,076 Page 11 Art Unit: 1751 Application/Control Number: 18/288,076 Page 12 Art Unit: 1751
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